Unterschiede

Hier werden die Unterschiede zwischen zwei Versionen der Seite angezeigt.

Link zu der Vergleichsansicht

Beide Seiten, vorherige ÜberarbeitungVorherige Überarbeitung
reactorgb [2026/03/22 02:44] – [Replacement of the reactor loading] administratorreactorgb [2026/03/24 17:57] (aktuell) – [Replacement of the reactor loading] administrator
Zeile 145: Zeile 145:
 </figure> </figure>
  
-After this prepare the new reactor loading. Usually the manufacturers of the boxes will provide refill sets for your specific systems ({{ref>refill_a}}). In this case there are two bags of molecular sieves, one bag of catalyst and two rubber gaskets for the meshed sealing rings ({{ref>refill_b}}). Replace the gaskets. To refill the reactor a suitable funnel is needed. For this purpose I 3D-printed a funnel with a KF40 flange which can be directly mounted onto the reactor ({{ref>refill_c}}). The model is provided [[https://www.thingiverse.com/thing:7319176|here]]. Mount the funnel on the same flange where the old loading came out. Refill the reactor in a specific order: First a bag of molecular sieves, then the bag with the catalyst and lastly the second bag with molecular sieves. The reason for this order is that the catalyst would be packed between the molecular sieves and therefore additionally protected. Now that the loading is replaced everything needs to be put together in reversed order.+After this prepare the new reactor loading. Usually the manufacturers of the boxes will provide refill sets for your specific systems ({{ref>refill_a}}). In this case there are two bags of molecular sieves, one bag of catalyst and two rubber gaskets for the meshed sealing rings ({{ref>refill_b}}). Replace the gaskets. To refill the reactor a suitable funnel is needed. For this purpose I 3D-printed a funnel with a KF40 flange which can be directly mounted onto the reactor ({{ref>refill_c}}). The model is provided [[https://www.thingiverse.com/thing:7319176|here (external link)]]. Mount the funnel on the same flange where the old loading came out. Refill the reactor in a specific order: First a bag of molecular sieves, then the bag with the catalyst and lastly the second bag with molecular sieves. The reason for this order is that the catalyst would be packed between the molecular sieves and therefore additionally protected. Now that the loading is replaced everything needs to be put together in reversed order.