Dies ist eine alte Version des Dokuments!


Elemental analysis

To prepare samples for elemntal analysis of sensitive compounds inside a glove box small capsules made out of tin proved to be reliable.

title
(a)
 title
(b)
 title
(c)

Figure 1: Capsules made out of tin for elemental analysis.

For the ease of taking pictures the process of how to prepare a sample is shown outside a glove box. The capsules are tiny and relatively soft. Therefore some custom tools are needed to prepare them inside a glove box.

title
(a)
 title
(b)
 title
(c)
 title
(d)

Figure 2: Tools recommended to prepare a sample.

Use the pointy tweezer to place one capsule into the holder. The holder is just a small piece of metal or polymer with a small hole for the capsule (dimensions of the capsules: 3.5×7 mm). I also created a 3D printable model here.

title
(a)
 title
(b)

Figure 3: Place the capsule into the holder using the pointy tweezer.